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Development and characterisation of soft magnetic iron-silicon alloys for laser beam powder bed fusion additive manufacturing

datacite.subject.fosCiências Naturais::Ciências Físicaspt_PT
dc.contributor.advisorEvans, Guiomar Gaspar de Andrade
dc.contributor.advisorBatalha, Rodolfo Lisboa
dc.contributor.authorFeliciano, Francisco Ramos
dc.date.accessioned2023-12-27T14:20:16Z
dc.date.available2023-12-27T14:20:16Z
dc.date.issued2023
dc.date.submitted2023
dc.descriptionTese de Mestrado, Engenharia Física, 2023, Universidade de Lisboa, Faculdade de Ciênciaspt_PT
dc.description.abstractWith the constant increase of global warming and the electric transition in the transportation industry, improving the efficiency and reducing the power losses of soft magnetic materials is mandatory. This work investigated the Fe-Si alloys production with the additive manufacturing technology Powder Bed Fusion - Laser Beam (PBF-LB). This soft magnetic material has many applications on electric machines. Like all the additive manufacturing techniques, layer-by-layer productions, the PBF-LB is characterised by melting a layer of powder with a laser beam in the desired regions, allowing a big design freedom. The main objective is to produce samples of Fe-3.5Si and Fe-6.5Si with PBF-LB, optimising the process parameters for each alloy to obtain the highest relative density and less surface roughness. Every built sample is post-processed and prepared for microscopy observation. Several heat treatments are also applied to understand the effects of the stress relief and grain growth on the final properties. The final procedure is the measure of magnetic properties, hardness values and grain size and shape. The magnetic properties and hardness values measured on Fe-3.5Si alloys indicate a dependence on the production scanning pattern and the posterior heat treatment applied in the samples. Samples with higher relative densities and less surface roughness are observed to reach higher magnetic permeabilities and inductions, and smaller coercivities, leading to fewer hysteresis losses. After a recrystallisation annealing heat treatment, the samples have improved their overall magnetic properties. It is observed that the hardness of the samples decreases with the heat treatments. The Fe-6.5Si alloys reach better magnetic properties than the previous alloy, being crack susceptible due to the formation of ordered phases. It is concluded that Fe-Si alloys produced with additive manufacturing achieve good results, but these materials could have even better magnetic properties (fewer losses and higher efficiencies) by removing the cracks and controlling the microstructure orientation. The changes in the production process or chemical composition of high silicon alloys can help reduce the cracking and reach denser samples.pt_PT
dc.identifier.tid203525159
dc.identifier.urihttp://hdl.handle.net/10451/61544
dc.language.isoengpt_PT
dc.subjectFabrico Aditivopt_PT
dc.subjectFusão em camada de pó com feixe laserpt_PT
dc.subjectMateriais magnéticos maciospt_PT
dc.subjectLigas de ferro silíciopt_PT
dc.subjectPropriedades magnéticaspt_PT
dc.subjectTeses de mestrado - 2023pt_PT
dc.titleDevelopment and characterisation of soft magnetic iron-silicon alloys for laser beam powder bed fusion additive manufacturingpt_PT
dc.typemaster thesis
dspace.entity.typePublication
rcaap.rightsopenAccesspt_PT
rcaap.typemasterThesispt_PT
thesis.degree.nameMestrado em Engenharia Físicapt_PT

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